{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"由甲基丙烯酸甲酯(MMA)、丙烯酸丁酯(BA)和含氟丙烯酸酯合成了含氟三元共聚乳液. FT-IR、1H NMR、13C NMR和19F NMR对产物的组成和结构进行了分析. 研究了含氟单体用量、增溶剂β-环糊精(β-CD)用量和聚合条件对乳液聚合动力学、粒径和粒径分布的影响,以及这些因素对三元共聚物性能的影响. 结果表明,聚合反应温度在55～65 ℃范围,升高温度,使聚合反应速率明显加快. 热分析表明,聚合温度对共聚物的组成几乎没有影响. 增加含氟单体用量(摩尔分数0～3.0%),使聚合反应速率略有降低.加入少量增溶剂β-CD使共聚物的玻璃化温度(Tg)升高. 与不含氟的共聚物 P(MMA-co-BA) 膜性能比较,三元含氟共聚物乳液涂膜的表面接触角明显增大,表明共聚物中具有含氟结构单元有利于提高膜性质.","authors":[{"authorName":"<span style=\"color:red\">纪</span><span style=\"color:red\">晓</span><span style=\"color:red\">丽</span>","id":"3e0957d9-5726-49b7-b89a-e5a24e53e3da","originalAuthorName":"纪晓丽"},{"authorName":"余樟清","id":"80341732-f220-4075-8eb0-17da62682914","originalAuthorName":"余樟清"},{"authorName":"倪沛红","id":"3805483f-855e-4a8d-a165-ddc09701bc09","originalAuthorName":"倪沛红"},{"authorName":"邵亚军","id":"c8f54c91-051a-46e1-b764-6eabd696c6f0","originalAuthorName":"邵亚军"}],"doi":"10.3969/j.issn.1000-0518.2004.09.005","fpage":"890","id":"9b9f031d-0d99-43d5-8bec-61a1a24dbacb","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9c0b6349-a0e9-46e8-b70d-e534f558f89e","keyword":"甲基丙烯酸甲酯","originalKeyword":"甲基丙烯酸甲酯"},{"id":"9c070e7c-d738-4d2c-99db-f80c9aa15c90","keyword":"丙烯酸丁酯","originalKeyword":"丙烯酸丁酯"},{"id":"68966cfb-a593-48db-931e-13fd21ee22c4","keyword":"含氟甲基丙烯酸酯","originalKeyword":"含氟甲基丙烯酸酯"},{"id":"b1b1a727-b8c0-4aea-824e-352dd2b4df0d","keyword":"β-环糊精","originalKeyword":"β-环糊精"},{"id":"47a99bf9-040b-4d7d-b466-7e59641f8288","keyword":"乳液共聚物","originalKeyword":"乳液共聚物"}],"language":"zh","publisherId":"yyhx200409005","title":"含氟三元丙烯酸酯乳液共聚物的合成及性能","volume":"21","year":"2004"},{"abstractinfo":"本刊2012年第五期第801页刊登了熊<span style=\"color:red\">晓</span>英等作者的论文,这是本刊编辑部自创刊以来收到的第一篇这样的论文,该文对本刊在材料科学期刊中所处的地位及面临问题、发展方向作出如此客观、中肯的评价与指引,均使编辑部成员十分感动。今年恰是本刊创刊30周年纪念,谨以此《编后记》供奉广大读者,","authors":[{"authorName":"无","id":"6eb4c714-a474-4cd0-b393-f0306b138318","originalAuthorName":"无"}],"doi":"","fpage":"714","id":"70565a37-1b6d-4b46-9b09-eb71030a22e8","issue":"5","journal":{"abbrevTitle":"CLKXYGCXB","coverImgSrc":"journal/img/cover/CLKXYGCXB.jpg","id":"13","issnPpub":"1673-2812","publisherId":"CLKXYGCXB","title":"材料科学与工程学报"},"keywords":[{"id":"b4b988f9-967f-4530-817f-d29f1623cfa2","keyword":"科学评价","originalKeyword":"科学评价"},{"id":"614f8cc5-6336-4065-b303-26b67f81d1be","keyword":"论文","originalKeyword":"论文"},{"id":"bf3cdaa0-4927-4d1a-a122-779ead854c34","keyword":"作者","originalKeyword":"作者"},{"id":"54d5797b-6f47-4f76-9527-3b32105f0299","keyword":"务实","originalKeyword":"务实"},{"id":"2124d564-90da-4a58-85da-22654e0d5dd2","keyword":"科学期刊","originalKeyword":"科学期刊"},{"id":"1dee1687-be42-4d28-aed7-6cd29a5c6883","keyword":"编辑部","originalKeyword":"编辑部"},{"id":"b28e651a-8495-4eba-87c6-79d47b81d924","keyword":"创刊","originalKeyword":"创刊"}],"language":"zh","publisherId":"clkxygc201205014","title":"科学评价,务实求真——熊<span style=\"color:red\">晓</span>英等作者的论文编后记","volume":"30","year":"2012"},{"abstractinfo":"对<span style=\"color:red\">丽</span>文哈贝壳的微结构进行了扫描电镜(SEM)观察,观察显示它是由无机霰石层和有机胶原蛋白组成的一种生物陶瓷复合材料,其中无机霰石层平行于贝壳表面整齐排列.观察也显示这些霰石层是由长而薄的霰石片所组成,不同霰石层中的霰石片具有不同的方向,构成螺旋等铺层形式.更仔细的观察显示每一霰石片又是由长而细的霰石纤维所组成,最细的霰石纤维具有纳米的尺度.根据在贝壳中观察到的螺旋结构,进行了螺旋结构和平行结构最大拔出力的比较实验研究,结果显示螺旋结构的最大拔出力大于平行结构的最大拔出力,它使贝壳具有高的强韧性.研究结果对高性能仿生陶瓷复合材料设计提供了有益指导.","authors":[{"authorName":"陈斌","id":"91984828-0e77-4a93-8cfd-2a46e2d25fed","originalAuthorName":"陈斌"},{"authorName":"彭向和","id":"d5ef20d1-e4e5-4a98-ba6b-92196ea2e073","originalAuthorName":"彭向和"},{"authorName":"孙士涛","id":"75180f74-ebf9-43d4-8789-47a26820e62b","originalAuthorName":"孙士涛"},{"authorName":"季金苟","id":"40f27576-f5ed-4e6e-b90d-d14547d07392","originalAuthorName":"季金苟"},{"authorName":"陈松","id":"964db22e-7bbb-4c54-80ae-5085d2652f09","originalAuthorName":"陈松"}],"doi":"","fpage":"60","id":"3b75f394-59d0-43b2-a932-20048ca15d0a","issue":"z1","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"27c2d5d0-a910-4ad5-877a-f290d9c33e02","keyword":"<span style=\"color:red\">丽</span>文哈贝壳","originalKeyword":"丽文哈贝壳"},{"id":"9b386643-5818-48f6-b972-95cb3df8690a","keyword":"生物陶瓷复合材料","originalKeyword":"生物陶瓷复合材料"},{"id":"1282b5cd-aa58-48ae-816f-8792bfb44248","keyword":"螺旋微结构","originalKeyword":"螺旋微结构"},{"id":"aadcdba1-cd86-4a6e-839e-1b9c5dec2ce3","keyword":"最大拔出力","originalKeyword":"最大拔出力"}],"language":"zh","publisherId":"xyjsclygc2008z1015","title":"<span style=\"color:red\">丽</span>文哈贝壳螺旋微结构研究","volume":"37","year":"2008"},{"abstractinfo":"在美国第45届材料与加工工程促进学会年会与展览共有世界上著名的八家碳纤维公司展出了碳纤维及其复合材料产品。本文简要介绍日本东<span style=\"color:red\">丽</span>公司碳纤维及其复合材料制品的新发展。","authors":[{"authorName":"赵稼祥","id":"c79e9472-89e1-4a86-be9f-d0deaa465bd5","originalAuthorName":"赵稼祥"}],"doi":"10.3969/j.issn.1007-2330.2000.06.013","fpage":"53","id":"98409ab3-a933-4c96-b40f-c323ad8736ff","issue":"6","journal":{"abbrevTitle":"YHCLGY","coverImgSrc":"journal/img/cover/YHCLGY.jpg","id":"77","issnPpub":"1007-2330","publisherId":"YHCLGY","title":"宇航材料工艺   "},"keywords":[{"id":"9459c9a0-2afa-47bc-b809-825ea01b1cff","keyword":"碳纤维","originalKeyword":"碳纤维"},{"id":"69e651c4-aaad-4ba6-9b00-4f643a730b19","keyword":"复合材料","originalKeyword":"复合材料"},{"id":"db524200-8c29-4cd5-a20f-a7fd2c10a480","keyword":"东<span style=\"color:red\">丽</span>公司","originalKeyword":"东丽公司"}],"language":"zh","publisherId":"yhclgy200006013","title":"东<span style=\"color:red\">丽</span>公司碳纤维及其复合材料的进展","volume":"30","year":"2000"},{"abstractinfo":"利用铱催化高碘酸钾氧化<span style=\"color:red\">丽</span>春红G(PG)的褪色反应,建立了测定痕量铱的催化动力学光度法.在硫酸介质和90℃加热15min的条件下,于500nm波长处,采用固定时间法测定<span style=\"color:red\">丽</span>春红G吸收值的降低.Ir(Ⅳ)的浓度在0～1.0μg/25mL范围内与催化反应的速率有良好的线性关系,检出限为1 81 ×10 mg/mL.对0.3μg/25mLIr(Ⅳ)测定的相对标准偏差为1.61%(n=11).体系至少稳定3.5h.考察了40多种共存离子的影响,大多数常见离子不干扰,方法有较好的选择性.催化反应对Ir(Ⅳ)和<span style=\"color:red\">丽</span>春红G均为一级反应,催化反应的表观活化能为103.66kJ/mol.用于冶金产品及岩矿中铱的测定,结果与推荐值十分吻合.","authors":[{"authorName":"侯能邦","id":"92c62fdf-fec8-4163-aad2-9ed54b7fdce6","originalAuthorName":"侯能邦"},{"authorName":"李祖碧","id":"c4dacfbe-4824-4cbe-a844-91a76be4f69c","originalAuthorName":"李祖碧"},{"authorName":"李崇宁","id":"f7a10f8c-895c-486c-ad99-2b32db2c7164","originalAuthorName":"李崇宁"},{"authorName":"王加林","id":"6d15967f-b1aa-492c-9003-5900696277f5","originalAuthorName":"王加林"},{"authorName":"曹秋娥","id":"b89522cc-6338-40b9-bb28-a8fc73f09d40","originalAuthorName":"曹秋娥"}],"doi":"10.3969/j.issn.1000-7571.2002.05.006","fpage":"17","id":"cf8ee9a7-e782-4fcb-866c-e15d9126e60f","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"3c381e65-e813-4912-b9c8-15299a341a75","keyword":"铱","originalKeyword":"铱"},{"id":"90683ee6-f835-43a8-b573-bc0be1641329","keyword":"<span style=\"color:red\">丽</span>春红G","originalKeyword":"丽春红G"},{"id":"a2a57fdf-fa6d-4d5d-bc97-967b1b2de292","keyword":"高碘酸钾","originalKeyword":"高碘酸钾"},{"id":"4ffcfe3c-3af4-41cd-ae8f-447d4f037585","keyword":"催化光度法","originalKeyword":"催化光度法"}],"language":"zh","publisherId":"yjfx200205006","title":"高碘酸钾氧化<span style=\"color:red\">丽</span>春红G催化光度法测定铱","volume":"22","year":"2002"},{"abstractinfo":"涂装的质量提高和生产成本的降低,可为机电产品制造领域创造附加值,还可以增加市场竞争力,所以人们对21世<span style=\"color:red\">纪</span>新型涂料开发、涂装作业方式改变、劳动条件改善、涂装工艺技术装备改进、开发等等都抱有很大的期望.全世界对公害和地球暖化等问题更加关心,环保问题是涂装行业最大的问题.涂料、涂装设备、涂装应用三位一体共同合作,是21世<span style=\"color:red\">纪</span>达到无公害涂装要取得成效的重要一步.我国机械制造大型企业在加强科研开发力量的同时不要忽视涂装技术这一重要领域.","authors":[],"doi":"","fpage":"65","id":"b1f1f25d-8e1c-4d6a-a107-e2331ba8a316","issue":"1","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"7a805d76-ec46-4830-8ce4-7f34b9ab216d","keyword":"涂料","originalKeyword":"涂料"},{"id":"1785eda3-238e-4b47-ba14-979aa0b2c04d","keyword":"涂装","originalKeyword":"涂装"},{"id":"f9f24383-5eff-4b55-9bc6-5a9d7f83b347","keyword":"装备","originalKeyword":"装备"},{"id":"28f7663e-ee5d-466d-ae50-c1b7704b74cc","keyword":"开发","originalKeyword":"开发"},{"id":"d1c84c05-b0e8-407d-8da2-4453b33856cd","keyword":"展望","originalKeyword":"展望"}],"language":"zh","publisherId":"clbh200001021","title":"21世<span style=\"color:red\">纪</span>工业涂装展望","volume":"33","year":"2000"},{"abstractinfo":"21世<span style=\"color:red\">纪</span>迷你冷轧(Minicold 21TM)型冷轧厂--体现冷轧高附加值扁平产品的柔性生产概念.为了高效生产冷轧、镀锌以及彩涂扁平产品,达涅利威恩联合公司开发了称为\"21世<span style=\"color:red\">纪</span>迷你冷轧(Minicold 21TM)\"冷轧工艺.其最简单的形式包括1条推拉式酸洗线、1台单机架或双机架可逆冷轧机、批示退火、1台平整机和1台可配置在线彩涂的热浸镀锌.讨论了21世<span style=\"color:red\">纪</span>迷你冷轧(Minicold 21TM)型冷轧厂的技术特点并根据预计资本投资和转换成本以及产出产品市场价格进行了经济效益分析.分析说明在大多数情况下大约年产量50万t的冷轧厂能够产生经济效益.","authors":[{"authorName":"","id":"0fada555-8860-4b12-9d65-8fc934a96846","originalAuthorName":""}],"doi":"","fpage":"36","id":"3ea672c8-f83c-4b1c-ae55-1cc6818fd12f","issue":"2","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"d61e4642-9d20-4641-8705-dd2a0a97d0ce","keyword":"21世<span style=\"color:red\">纪</span>","originalKeyword":"21世纪"},{"id":"ef176028-d23c-4cbc-83be-a0af90e3250b","keyword":"迷你冷轧","originalKeyword":"迷你冷轧"}],"language":"zh","publisherId":"gt200402010","title":"迷你冷轧--21世<span style=\"color:red\">纪</span>冷轧技术","volume":"39","year":"2004"},{"abstractinfo":"21世<span style=\"color:red\">纪</span>冶金分析面临复杂体系痕量元素分析、原位状态定量分析(OPA)以及在线实时分析等三大问题.而炼钢过程熔融金属在线分析更是其中最具意义的难点.在展望其可能的研究方向的同时,评述了钢液直接分析技术.","authors":[{"authorName":"王海舟","id":"c35d3ed5-cffd-474f-8fe2-d2c4db298aa1","originalAuthorName":"王海舟"}],"doi":"","fpage":"73","id":"25114f57-8df3-4b20-83e6-f35bd5323296","issue":"1","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"39d0ebe0-0203-4f88-b1ab-bf4c9e21fb81","keyword":"冶金分析","originalKeyword":"冶金分析"},{"id":"b6ea80a1-3d7a-42c4-98e2-a7812c2c3a83","keyword":"痕量分析","originalKeyword":"痕量分析"},{"id":"8a034fb3-cba8-470f-8ffe-4fca7b6b09df","keyword":"原位状态分析","originalKeyword":"原位状态分析"},{"id":"b1b40503-6b17-4c39-9951-28bfe46f5815","keyword":"在线实时分析","originalKeyword":"在线实时分析"}],"language":"zh","publisherId":"gt200001019","title":"21世<span style=\"color:red\">纪</span>冶金分析的若干问题","volume":"35","year":"2000"},{"abstractinfo":"在阐述21世<span style=\"color:red\">纪</span>初汽车生产市场规模和环保法规基础上,介绍了环保型汽车涂料发展趋势和减少CO2排放及节能措施.讲述了关西涂料公司在这方面所取得的技术进步及设想.","authors":[{"authorName":"关文斌","id":"022d71b0-3dba-42fd-9112-854956b7aedb","originalAuthorName":"关文斌"},{"authorName":"粘林正明","id":"03c306c1-86b9-4d09-96fb-b9b3804d21e5","originalAuthorName":"粘林正明"}],"doi":"10.3969/j.issn.0253-4312.2000.11.003","fpage":"6","id":"41ae2f68-6530-4eca-a217-213aa1ee6419","issue":"11","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业   "},"keywords":[{"id":"eed72422-ebf4-4656-94eb-4a0c9fbd98c0","keyword":"汽车涂料","originalKeyword":"汽车涂料"},{"id":"0bd67ecf-fa4c-4066-b1d9-f19e45cc86fe","keyword":"环境保护","originalKeyword":"环境保护"},{"id":"b4f144b8-93c1-45e0-b295-8a2561ba8592","keyword":"节能","originalKeyword":"节能"},{"id":"f43d0907-7e02-42ec-b1f4-ed842b8d9d65","keyword":"低VOC","originalKeyword":"低VOC"}],"language":"zh","publisherId":"tlgy200011003","title":"21世<span style=\"color:red\">纪</span>汽车漆发展方向","volume":"30","year":"2000"},{"abstractinfo":"从漆前处理技术、阴极电泳涂装技术、膜过滤技术、自动静电涂装技术、静电粉末涂装技术、烘干技术、汽车用涂料和涂装管理等8个方面围绕环保、高质量、降成本3个主题,展望21世<span style=\"color:red\">纪</span>汽车涂装的发展趋势.","authors":[],"doi":"","fpage":"61","id":"8ab7d74e-24bc-4708-b117-203c70f670d5","issue":"1","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"45580757-9a69-45bd-9f41-639d5a64b9be","keyword":"21世<span 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