{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":4,"startPagecode":1},"records":[{"abstractinfo":"采用焙烧酸处理成功制备了酸化硅酸镁吸附材料,通过傅里叶红外(FT-IR)、扫描电镜(SEM)和全自动化表面积和孔结构分析仪等手段对样品结构进行表征;研究了酸化硅酸镁的吸附性能,考察了吸附剂加量、pH值、温度和时间等因素对稠油污水中有机物的吸附影响.结果表明,酸化处理改变了硅酸镁表面晶体结构,微孔数量与比表面积增加;强化了硅酸镁对稠油污水的有机物吸附,将同浓度的COD去除率从52.94%提高到76.12%;吸附剂的吸附能力随温度的升高而降低;强酸或强碱性条件下有利于对稠油污水中有机物的吸附;吸附0.5 h,COD去除率可达65.58%.","authors":[{"authorName":"杜国勇","id":"031925a0-540e-4517-a012-c529fbdedbad","originalAuthorName":"杜国勇"},{"authorName":"张洪铭","id":"936d888e-dd96-412f-99db-2f08073e91ca","originalAuthorName":"张洪铭"},{"authorName":"李艳","id":"93ecd5cc-db7f-4a41-ba50-d999cf6d3b33","originalAuthorName":"李艳"},{"authorName":"<span style=\"color:red\">邓</span><span style=\"color:red\">春</span><span style=\"color:red\">萍</span>","id":"7a49e642-ccbe-4463-976e-74e560d1fd81","originalAuthorName":"邓春萍"},{"authorName":"汪倩","id":"e8cfe923-64ac-4892-afd4-94dacf114a0b","originalAuthorName":"汪倩"},{"authorName":"朱盟翔","id":"572abd6f-6e67-4d28-b0af-18bd5dbad521","originalAuthorName":"朱盟翔"}],"doi":"10.3969/j.issn.1001-9731.2017.06.003","fpage":"6013","id":"bcd60bf1-4269-4ecc-8767-95a45d3efbbe","issue":"6","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"c08e5adb-9c78-479c-a465-9d125f5a440c","keyword":"硅酸镁","originalKeyword":"硅酸镁"},{"id":"6e58ed80-fb7b-49fa-88e1-02e34c9ef106","keyword":"酸化","originalKeyword":"酸化"},{"id":"a3b3df58-2e9e-4536-bcbe-4f01ace63b91","keyword":"稠油污水","originalKeyword":"稠油污水"},{"id":"4b07dda9-2023-4d5b-ae1a-f755c856c6b4","keyword":"吸附","originalKeyword":"吸附"}],"language":"zh","publisherId":"gncl201706003","title":"硅酸镁的改性及其对稠油污水中有机物的吸附","volume":"48","year":"2017"},{"abstractinfo":"采用Chiralpak IC手性柱(250 mm×4.6 mm,5 μm),建立了正相高效液相色谱测定板蓝根中表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)和告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)含量的方法.考察了流动相组成、流速和柱温对分离度的影响.经优化后的实验条件:以正己烷-异丙醇(体积比为90∶10)为流动相,流速为0.8 mL/min;检测波长为245 nm,柱温为20 ℃.在此优化条件下,表告依<span style=\"color:red\">春</span>和告依春分离度为3.4,检出限为2.0 mg/L,在0.02～2.0 g/L 范围内有良好的线性关系,平均回收率为101% ,相对标准偏差(RSD)小于3.0%(n=6).本方法可将具有抗病毒活性的表告依<span style=\"color:red\">春</span>与其对映体告依<span style=\"color:red\">春</span>基线分离并测定,专属性强,能有效控制板蓝根的质量.","authors":[{"authorName":"聂黎行","id":"fee7f0b1-4bfd-4c4e-9d65-d7f03c2a918a","originalAuthorName":"聂黎行"},{"authorName":"王钢力","id":"ee281225-e77f-4477-a486-a098ca91b1db","originalAuthorName":"王钢力"},{"authorName":"戴忠","id":"813e1426-d061-4e41-9723-d75cfa16968e","originalAuthorName":"戴忠"},{"authorName":"林瑞超","id":"3034f33a-eaf2-4665-8751-f5ef70c65379","originalAuthorName":"林瑞超"}],"doi":"10.3724/SP.J.1123.2010.01001","fpage":"1001","id":"32355b8f-ccce-4726-b210-eaacc0917986","issue":"10","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"5c41c71f-d053-43ba-8aa9-32ad96d3cca4","keyword":"手性高效液相色谱法","originalKeyword":"手性高效液相色谱法"},{"id":"e26a591e-56ec-4bb4-acfd-5d5f7ad919ea","keyword":"表告依<span style=\"color:red\">春</span>(R-告依<span style=\"color:red\">春</span>)","originalKeyword":"表告依春(R-告依春)"},{"id":"1e32ab35-876b-46d9-9898-47fb5c40d701","keyword":"告依<span style=\"color:red\">春</span>(S-告依<span style=\"color:red\">春</span>)","originalKeyword":"告依春(S-告依春)"},{"id":"8c1b4600-8fac-47f6-98f6-6670e2a0daa9","keyword":"板蓝根","originalKeyword":"板蓝根"}],"language":"zh","publisherId":"sp201010018","title":"手性高效液相色谱法测定板蓝根中表告依<span style=\"color:red\">春</span>和告依<span style=\"color:red\">春</span>含量","volume":"28","year":"2010"},{"abstractinfo":"李绍宏,<span style=\"color:red\">邓</span>黎辉,谢殷子,吴晓<span style=\"color:red\">春</span>","authors":[{"authorName":"高碳高合金马氏体钢回火过程连续性转变的内耗行为研究","id":"a56d0ae1-54be-47af-858b-f74c82608c9c","originalAuthorName":"高碳高合金马氏体钢回火过程连续性转变的内耗行为研究"}],"categoryName":"|","doi":"","fpage":"37","id":"7cbdd3ec-863c-45d4-97c4-bdc3ee0336c9","issue":"4","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"59175031-3448-441b-b9cc-5e1c4d34ea4d","keyword":"高碳高合金马氏体钢淬火后在回火过程中存在过饱和碳原子偏聚现象，碳原子偏聚于位错附近的间隙位置，回火过程中以碳化物形式沉淀析出。通过内耗研究表明，随着回火温度的增加，Snoek峰驰豫强度下降并消失，SKK峰驰豫强度降低并随回火温度的升高而宽化。由该结果可知由于大量碳原子偏聚于位错处，随后以细颗粒碳化物形式在位错处析出。随着回火温度增加，大部分位错回复消失及碳化物聚集长大，同时残余奥氏体分解产生硬化效应，使钢的硬度增加而韧性下降。","originalKeyword":"高碳高合金马氏体钢淬火后在回火过程中存在过饱和碳原子偏聚现象，碳原子偏聚于位错附近的间隙位置，回火过程中以碳化物形式沉淀析出。通过内耗研究表明，随着回火温度的增加，Snoek峰驰豫强度下降并消失，SKK峰驰豫强度降低并随回火温度的升高而宽化。由该结果可知由于大量碳原子偏聚于位错处，随后以细颗粒碳化物形式在位错处析出。随着回火温度增加，大部分位错回复消失及碳化物聚集长大，同时残余奥氏体分解产生硬化效应，使钢的硬度增加而韧性下降。"}],"language":"zh","publisherId":"1001-0963_2011_4_8","title":"高性能精品模具钢系列产品的研究与开发(20079~201012)","volume":"23","year":"2011"},{"abstractinfo":"利用铱催化高碘酸钾氧化丽<span style=\"color:red\">春</span>红G(PG)的褪色反应,建立了测定痕量铱的催化动力学光度法.在硫酸介质和90℃加热15min的条件下,于500nm波长处,采用固定时间法测定丽<span style=\"color:red\">春</span>红G吸收值的降低.Ir(Ⅳ)的浓度在0～1.0μg/25mL范围内与催化反应的速率有良好的线性关系,检出限为1 81 ×10 mg/mL.对0.3μg/25mLIr(Ⅳ)测定的相对标准偏差为1.61%(n=11).体系至少稳定3.5h.考察了40多种共存离子的影响,大多数常见离子不干扰,方法有较好的选择性.催化反应对Ir(Ⅳ)和丽<span style=\"color:red\">春</span>红G均为一级反应,催化反应的表观活化能为103.66kJ/mol.用于冶金产品及岩矿中铱的测定,结果与推荐值十分吻合.","authors":[{"authorName":"侯能邦","id":"92c62fdf-fec8-4163-aad2-9ed54b7fdce6","originalAuthorName":"侯能邦"},{"authorName":"李祖碧","id":"c4dacfbe-4824-4cbe-a844-91a76be4f69c","originalAuthorName":"李祖碧"},{"authorName":"李崇宁","id":"f7a10f8c-895c-486c-ad99-2b32db2c7164","originalAuthorName":"李崇宁"},{"authorName":"王加林","id":"6d15967f-b1aa-492c-9003-5900696277f5","originalAuthorName":"王加林"},{"authorName":"曹秋娥","id":"b89522cc-6338-40b9-bb28-a8fc73f09d40","originalAuthorName":"曹秋娥"}],"doi":"10.3969/j.issn.1000-7571.2002.05.006","fpage":"17","id":"cf8ee9a7-e782-4fcb-866c-e15d9126e60f","issue":"5","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"3c381e65-e813-4912-b9c8-15299a341a75","keyword":"铱","originalKeyword":"铱"},{"id":"90683ee6-f835-43a8-b573-bc0be1641329","keyword":"丽<span style=\"color:red\">春</span>红G","originalKeyword":"丽春红G"},{"id":"a2a57fdf-fa6d-4d5d-bc97-967b1b2de292","keyword":"高碘酸钾","originalKeyword":"高碘酸钾"},{"id":"4ffcfe3c-3af4-41cd-ae8f-447d4f037585","keyword":"催化光度法","originalKeyword":"催化光度法"}],"language":"zh","publisherId":"yjfx200205006","title":"高碘酸钾氧化丽<span style=\"color:red\">春</span>红G催化光度法测定铱","volume":"22","year":"2002"},{"abstractinfo":"在90 ℃水浴中,Co2+ 能催化铋酸钠氧化丽<span style=\"color:red\">春</span>红S褪色,据此建立了一种褪色光度法测定Co2+ 的新方法.Co2+在0～50 μg/mL范围内遵守比尔定律,表观摩尔吸光系数为1.814×103 L/(mol*cm),最大吸收波长为520 nm,该方法检出限为0.538 μg/mL.该方法用于测定锡-钴枪黑色合金镀液中钴的含量,结果令人满意.","authors":[{"authorName":"郭振良","id":"584bf7f2-7e7f-4127-ade6-2c272d72dfbf","originalAuthorName":"郭振良"},{"authorName":"唐清华","id":"9ce2a809-b843-4434-8e7c-dac0f58527cb","originalAuthorName":"唐清华"},{"authorName":"牟起娜","id":"d37d8b39-f7ec-454c-a7d0-cf3e62dd6762","originalAuthorName":"牟起娜"},{"authorName":"孙言志","id":"7c0484e8-9cab-4b29-a48b-4bcb2c838cd8","originalAuthorName":"孙言志"}],"doi":"10.3969/j.issn.1004-227X.2005.12.018","fpage":"63","id":"8c6b0946-37e5-47d0-aff4-bf52e1cf4d1a","issue":"12","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰   "},"keywords":[{"id":"f6c28cfe-17af-49c2-b37f-6d1108f657b6","keyword":"丽<span style=\"color:red\">春</span>红S","originalKeyword":"丽春红S"},{"id":"cde44370-4a27-46a1-9f05-62ccb3d33206","keyword":"褪色光度法","originalKeyword":"褪色光度法"},{"id":"e7ed13de-3a0a-4b14-b563-e2203460d95f","keyword":"合金镀液","originalKeyword":"合金镀液"},{"id":"6cccbb22-6b70-42fd-9eb3-d3701b2868e9","keyword":"钴","originalKeyword":"钴"}],"language":"zh","publisherId":"ddyts200512018","title":"丽<span style=\"color:red\">春</span>红S褪色光度法测定锡-钴合金镀液中的钴","volume":"24","year":"2005"},{"abstractinfo":"","authors":[{"authorName":"乔明华","id":"5549d4b2-a449-4c6a-ad22-e7067450c1d6","originalAuthorName":"乔明华"},{"authorName":"许国勤","id":"8041ba67-6bf8-47c4-8f5e-67dfa4107f01","originalAuthorName":"许国勤"},{"authorName":"范康年","id":"919dbe5d-6084-42e9-8455-32fee7f5c4c0","originalAuthorName":"范康年"}],"doi":"10.1016/S1872-2067(12)60594-4","fpage":"820","id":"407741a9-2b63-4067-9ea7-3b6a307b2984","issue":"5","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"10f61789-cfb7-4946-a098-b6e9bd490cc7","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"cuihuaxb201305002","title":"<span style=\"color:red\">邓</span>景发先生传略","volume":"34","year":"2013"},{"abstractinfo":"基于在盐酸介质中,La(Ⅲ)催化过氧化氢氧化丽<span style=\"color:red\">春</span>红(3-羟基-4-(2-磺基-4-[4-苯磺基偶氮]偶氮苯)-2,7-萘二磺酸钠)的褪色反应,建立了一个灵敏度高的测定痕量La(Ⅲ)的催化动力学光度分析法.讨论了酸度、试剂用量、温度、干扰离子等因素的影响;研究了反应的最佳条件;测定了一些动力学参数.催化反应的表观活化能为66.63 kJ/mol.该方法测定La(Ⅲ)的线性范围为0.08～1.6 μg/mL,检出限为0.045 μg/mL.不需要预先分离,可将本方法用于沙子样品中痕量镧的测定,回收率为96.0%～111.5%.","authors":[{"authorName":"柳玉英","id":"d9ec6bd0-d964-4e32-8771-27a252778c36","originalAuthorName":"柳玉英"},{"authorName":"张少全","id":"2b0fcf73-acc9-4fea-8b44-e5a50abeaf85","originalAuthorName":"张少全"}],"doi":"10.3969/j.issn.1000-7571.2007.12.017","fpage":"67","id":"e07dfa5a-d08b-4575-bb1f-6a72fddac954","issue":"12","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"9c1ba52e-d166-412f-b761-4d857c395e9c","keyword":"动力学光度法","originalKeyword":"动力学光度法"},{"id":"ef492496-134d-4429-9178-04a73e0cc88b","keyword":"丽<span style=\"color:red\">春</span>红","originalKeyword":"丽春红"},{"id":"b896c3e7-0783-4577-adb9-3d560b75ea51","keyword":"镧","originalKeyword":"镧"},{"id":"e334331e-4000-434a-8d11-a4d75c544c6c","keyword":"过氧化氢","originalKeyword":"过氧化氢"}],"language":"zh","publisherId":"yjfx200712017","title":"镧(Ⅲ)催化过氧化氢氧化丽<span style=\"color:red\">春</span>红褪色光度法测定痕量镧","volume":"27","year":"2007"},{"abstractinfo":"","authors":[{"authorName":"吴钰重","id":"9c027aa4-b103-451d-8e97-5f473eac2352","originalAuthorName":"吴钰重"}],"doi":"10.3969/j.issn.1000-6826.2015.05.01","fpage":"1","id":"0506a7f0-4c97-4d66-a669-f34c1c16bd2f","issue":"5","journal":{"abbrevTitle":"JSSJ","coverImgSrc":"journal/img/cover/3abe017a-2574-4821-8152-4ae974ef0471.jpg","id":"47","issnPpub":"1000-6826","publisherId":"JSSJ","title":"金属世界"},"keywords":[{"id":"d9b0bd3a-6769-4f19-8833-73a919a0d3ad","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"jssj201505001","title":"冯<span style=\"color:red\">春</span>：勤恳为师路，执着科研心","volume":"","year":"2015"},{"abstractinfo":"","authors":[{"authorName":"范康年","id":"58594def-046d-41fa-a0f0-d0679d6021cf","originalAuthorName":"范康年"},{"authorName":"包信和","id":"de540cf9-e151-4cf5-a7d2-b5c96c767eec","originalAuthorName":"包信和"},{"authorName":"许国勤","id":"5ffa3076-1e01-45fd-91be-8642c8eab334","originalAuthorName":"许国勤"}],"doi":"10.1016/S1872-2067(12)60593-2","fpage":"817","id":"a3f29cea-b852-44ec-bab0-86db75086298","issue":"5","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"1a505dad-952b-4673-a246-52a95132a30c","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"cuihuaxb201305001","title":"《催化学报》以本期专刊的出版纪念<span style=\"color:red\">邓</span>景发院士诞辰八十周年","volume":"34","year":"2013"},{"abstractinfo":"2004年上半年的钯市场为基金所主宰,价格出人意料地突破了300美元/盎司阻力线,收在18个月的高点.基本面虽然没有实质性的支撑,但未来需求的增长潜力大大鼓励了基金的热情.预计下半年的投机活力将有所减弱,基金有撤出商品市场的迹象.但价格处于历史低点、中长期需求看好的钯市场仍有吸引力,因此下半年的钯价仍将在投机的掌控之中.预计价格将在200美元/盎司处有强支撑,上行强阻在31 0～330美元/盎司区间;如果突破该价位,下一个阻力位将在370美元/盎司附近.","authors":[{"authorName":"靳湘云","id":"e350353d-3410-4148-bc78-c56e8c98c1b4","originalAuthorName":"靳湘云"}],"doi":"10.3969/j.issn.1674-3962.2004.08.005","fpage":"19","id":"71d445aa-a10f-45fb-8d62-c4c599bde8fd","issue":"8","journal":{"abbrevTitle":"ZGCLJZ","coverImgSrc":"journal/img/cover/中国材料进展.jpg","id":"80","issnPpub":"1674-3962","publisherId":"ZGCLJZ","title":"中国材料进展"},"keywords":[{"id":"bdc8b742-cce7-460a-b320-d1da28b4cf92","keyword":"钯市场","originalKeyword":"钯市场"},{"id":"f5636990-a8be-4bc4-9beb-ef07ccdb7de8","keyword":"半年","originalKeyword":"半年"},{"id":"81118ffe-6b3f-4337-836f-94830aa05765","keyword":"回顾","originalKeyword":"回顾"},{"id":"d491766d-30e0-4637-a07b-6055c51c4dc5","keyword":"展望","originalKeyword":"展望"}],"language":"zh","publisherId":"zgcljz200408005","title":"枯木逢<span style=\"color:red\">春</span>渐渐进--钯市场2004年上半年回顾与下半年展望","volume":"23","year":"2004"}],"totalpage":4,"totalrecord":33}