{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以2-氨基-5-烃基-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>和水杨醛为原料,分别用“分步法”和“一锅法”经还原中间产物Schiff碱的C=N双键合成了一系列2-((1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>基)<span style=\"color:red\">胺</span><span style=\"color:red\">甲基</span>)<span style=\"color:red\">苯酚</span>类新化合物,“一锅法”的产率较高,为56％～80％.产物的结构用IR、1H NMR、13C NMR和MS进行了表征.初步测试了目标化合物的杀菌活性,证明化合物对赤星病菌具有较好的抑菌活性,当浓度为25 mg/L时,化合物3i的抑制率为76％,化合物3f、3h、3k和3l的为70％.","authors":[{"authorName":"唐子龙","id":"bbc40a65-fe4c-4004-a72d-88c64b816e1c","originalAuthorName":"唐子龙"},{"authorName":"常书红","id":"a807d957-f5e6-4d43-afe4-57090e44bfc6","originalAuthorName":"常书红"},{"authorName":"颜林","id":"6004f211-df6c-4c83-becf-d6e50a80c456","originalAuthorName":"颜林"},{"authorName":"刘汉文","id":"7252df29-224f-48b0-ba50-4cdc59e2eaa9","originalAuthorName":"刘汉文"}],"doi":"10.3724/SP.J.1095.2012.00410","fpage":"878","id":"3fc7cc85-2753-47d0-b10f-73257d2d10f8","issue":"8","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"5cb60691-76e8-4b4e-ab12-8f557eed1313","keyword":"<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span><span style=\"color:red\">胺</span><span style=\"color:red\">甲基</span><span style=\"color:red\">苯酚</span>","originalKeyword":"噻二唑胺甲基苯酚"},{"id":"e76f9847-6b5f-4bdc-8d36-eeb7ec2aed81","keyword":"合成","originalKeyword":"合成"},{"id":"a81406b0-4809-4e6d-aabf-888dc2a590f9","keyword":"杀菌活性","originalKeyword":"杀菌活性"}],"language":"zh","publisherId":"yyhx201208005","title":"2-(1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span><span style=\"color:red\">胺</span><span style=\"color:red\">甲基</span>)<span style=\"color:red\">苯酚</span>的合成及其杀菌活性","volume":"29","year":"2012"},{"abstractinfo":"用循环伏安法研究了2,5-<span style=\"color:red\">二</span>巯基-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>(DMcT)/聚邻<span style=\"color:red\">甲基</span>苯胺(POT)复合电极的电化学特性. 结果表明,以铜为其集流体时电极有较好的电化学活性. 在DMcT/POT复合电极中,随电极中POT含量的增加,电极的电流效率上升,而复合电极的可逆性在m(DMcT)/m(POT)=1时较好.","authors":[{"authorName":"李朝晖","id":"2b6b9a5f-c6c6-49c2-9be1-6f470dcf9a66","originalAuthorName":"李朝晖"},{"authorName":"苏光耀","id":"1b827132-628f-41f0-a6d8-62cc80dd64ab","originalAuthorName":"苏光耀"},{"authorName":"王霞瑜","id":"4b228ed6-5562-4fa5-9874-8544603f5857","originalAuthorName":"王霞瑜"},{"authorName":"高德淑","id":"5c4f102c-d993-4020-a710-b362a6134ee5","originalAuthorName":"高德淑"},{"authorName":"雷钢铁","id":"365ef9e9-ee09-4450-a484-34da094b3c81","originalAuthorName":"雷钢铁"}],"doi":"10.3969/j.issn.1000-0518.2003.06.008","fpage":"542","id":"1b49c78d-4765-4ed2-9b76-d457a6ffa724","issue":"6","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"5f415f44-184d-44db-a488-8d82ba87237d","keyword":"有机<span style=\"color:red\">二</span>硫化合物","originalKeyword":"有机二硫化合物"},{"id":"97df2f89-474e-4d7b-b123-0a17b000551c","keyword":"<span style=\"color:red\">二</span>巯基<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"二巯基噻二唑"},{"id":"c907e16b-9c7f-44ec-af39-0b6fcae2b72e","keyword":"聚邻<span style=\"color:red\">甲基</span>苯胺","originalKeyword":"聚邻甲基苯胺"},{"id":"ee55ef26-12db-42f0-bcd8-b25ea291d00a","keyword":"锂电池","originalKeyword":"锂电池"}],"language":"zh","publisherId":"yyhx200306008","title":"2,5-<span style=\"color:red\">二</span>巯基-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>/聚邻<span style=\"color:red\">甲基</span>苯胺复合电极的电化学性能","volume":"20","year":"2003"},{"abstractinfo":"将2-巯基-5-取代基-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>经与β-氯苯丙酮取代、盐酸羟<span style=\"color:red\">胺</span>肟化和氯<span style=\"color:red\">甲基</span>(口恶)<span style=\"color:red\">二</span><span style=\"color:red\">唑</span>醚化,合成了6种3-(5-取代基-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>-2-硫代基)-1-苯基丙酮-O-(5-苯基-1,3,4-(口恶)<span style=\"color:red\">二</span><span style=\"color:red\">唑</span>-2-<span style=\"color:red\">甲基</span>)肟醚化合物(4a～4f),用1 H NMR、IR、MS和元素分析表征了其结构.用MTT法测试了6种目标化合物对人黑色素瘤细胞株B16、人白血病细胞株HL60和人肝癌细胞株SMMC-7721的体外细胞毒活性.测试结果表明,部分化合物对3种癌细胞具有潜在的体外生长抑制活性.","authors":[{"authorName":"张耀洲","id":"ab4c77b9-4773-4adc-b2cb-e1ad5a8ec6ba","originalAuthorName":"张耀洲"},{"authorName":"肖颖","id":"2ac64980-6e63-42ad-8e30-194291bfccbd","originalAuthorName":"肖颖"},{"authorName":"杨俊杰","id":"1555ecaf-5de8-435b-831c-afebe6f9cef8","originalAuthorName":"杨俊杰"},{"authorName":"胡国强","id":"d4c25027-c87a-4451-a428-33e87130e72a","originalAuthorName":"胡国强"}],"doi":"10.3724/SP.J.1095.2013.20259","fpage":"383","id":"8b57d618-2884-4f84-906c-cc1565aa6363","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"30532710-9893-4fb9-add5-0e19d821a2d8","keyword":"<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"噻二唑"},{"id":"ba41d2c4-fbb6-4f68-afb0-2170f3bf448d","keyword":"(口恶)<span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"(口恶)二唑"},{"id":"c6be7536-f0a0-4658-99c7-2aa3bb2e3729","keyword":"肟醚","originalKeyword":"肟醚"},{"id":"00fb2bd3-eba4-46ed-99ff-e1c09b1d1141","keyword":"抗肿瘤活性","originalKeyword":"抗肿瘤活性"}],"language":"zh","publisherId":"yyhx201304004","title":"肟醚<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>硫醚化合物的合成及其抗肿瘤活性","volume":"30","year":"2013"},{"abstractinfo":"利用电化学测试和表面分析技术,研究了2,5-<span style=\"color:red\">二</span>巯基-1,3,4<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>(DMTD)在硫-乙醇溶液中对金属银、铜的缓蚀性能,结合量子化学计算和分子动力学模拟对DMTD在金属表面的吸附行为和缓蚀作用机理进行了分析讨论.结果表明,DMTD在50 mg/L的硫-乙醇溶液中,对金属银、铜均起到较好的缓蚀作用.极化曲线结果表明,当缓蚀剂DMTD浓度达到50 mg/L时,缓蚀效率可以达到92.3%.表面分析技术表明,缓蚀剂的加入在金属表面形成吸附膜,明显抑制了腐蚀速率.量化计算和分子动力学模拟得到了缓蚀剂分子的活性位点和缓蚀剂在金属表面的吸附形态.","authors":[{"authorName":"刘琳","id":"38154dcf-5c81-43d6-bb02-5e8fce6358e6","originalAuthorName":"刘琳"},{"authorName":"彭丹","id":"0710a3eb-c895-438f-8f82-8d48279f8131","originalAuthorName":"彭丹"},{"authorName":"张艳萍","id":"7728b55a-e5a1-4815-8812-fc25df66a360","originalAuthorName":"张艳萍"},{"authorName":"刘娇","id":"19722010-c3d8-407a-92fd-5952958571bb","originalAuthorName":"刘娇"},{"authorName":"张强","id":"a5115812-fb28-4211-af4e-235bf921c077","originalAuthorName":"张强"},{"authorName":"钱建华","id":"b73253d8-0c01-48fd-8a9e-f4d74bee6fb6","originalAuthorName":"钱建华"}],"doi":"10.11896/j.issn.1005-023X.2016.06.019","fpage":"78","id":"f32e463b-621b-49db-8068-5b4c2c7892a1","issue":"6","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"b449a625-1617-4ffd-b16a-9e3740608e0e","keyword":"<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"噻二唑"},{"id":"23a454d7-a3c4-4349-9554-e54469d21b40","keyword":"极化曲线","originalKeyword":"极化曲线"},{"id":"30790105-dc45-4b87-9942-2b6866d1e77b","keyword":"分子动力学模拟","originalKeyword":"分子动力学模拟"}],"language":"zh","publisherId":"cldb201606020","title":"<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>型缓蚀剂缓蚀性能的研究","volume":"30","year":"2016"},{"abstractinfo":"利用活性亚结构拼接原理,将活性基团分别引入1,2,4-均三<span style=\"color:red\">唑</span>并[3,4-b]-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>杂环的3位和6位,合成了11种3,6-<span style=\"color:red\">二</span>取代均三<span style=\"color:red\">唑</span>并[3,4-b]-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>类新化合物,收率为43%～95%. 并用IR、1H NMR、EI-MS及元素分析测试技术对其进行了结构表征. 抑菌活性测试表明,所合成的大部分化合物对黄瓜灰霉病菌(Botrytis cinerea)有较好的生长抑制作用,其中,化合物5ae、5ag和5bd的抑制率均达70%,化合物5ad、5cd、5ce的抑制率大于60%,化合物5bd对水稻纹枯病菌(Pellicularia sasakii)抑制率大于60%,化合物5cg对西瓜炭疽病菌(Colletotrichum lagenarium)的抑制率为69%.","authors":[{"authorName":"杨知昆","id":"53a41908-d645-479d-b974-9f622f0d8c1a","originalAuthorName":"杨知昆"},{"authorName":"孙学军","id":"a87abf68-14c1-433e-a764-ba84876bdf31","originalAuthorName":"孙学军"},{"authorName":"米娜","id":"5288e279-b16e-4a2b-a306-7905f4f9c6b8","originalAuthorName":"米娜"},{"authorName":"张海科","id":"4713867d-240c-4de4-b91e-958509f32ff8","originalAuthorName":"张海科"},{"authorName":"尤进茂","id":"be248cf8-ca51-4b83-84c5-9488f6ee6ce6","originalAuthorName":"尤进茂"},{"authorName":"范志金","id":"78b01514-1b83-4dbc-b267-1c02b68ff628","originalAuthorName":"范志金"}],"doi":"10.3969/j.issn.1000-0518.2009.09.006","fpage":"1027","id":"f6f7382f-5e9d-493f-85b1-34d617512f9a","issue":"9","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"9eafc0c2-c046-4426-b1dd-fccfc9e2fd21","keyword":"均三<span style=\"color:red\">唑</span>并<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"均三唑并噻二唑"},{"id":"71e7f828-dffd-45e9-8aab-9b934365c0b8","keyword":"3-6位取代衍生物","originalKeyword":"3-6位取代衍生物"},{"id":"4081fe52-350e-4971-a25a-ea97d8c07d0b","keyword":"合成","originalKeyword":"合成"},{"id":"c313c0d7-c256-4c10-b41d-599fc02ff522","keyword":"杀菌活性","originalKeyword":"杀菌活性"}],"language":"zh","publisherId":"yyhx200909006","title":"三<span style=\"color:red\">唑</span>并<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>衍生物的合成及抑菌活性","volume":"26","year":"2009"},{"abstractinfo":"合成了两个系列以1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>为中心基团的弯曲型分子,结合偏光显微熔点仪(POM)观察和差示量热扫描法(DSC)研究了它们的液晶性能.研究发现,这两类弯曲型分子都会出现N相.其中,对称型五环酯类<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>弯曲型分子的熔点都较高,清亮点均超过360℃；含烯丙基非对称<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>类弯曲型分子熔点和清亮点温度大幅度降低,N相的温区较宽,以庚基为端基链的弯曲型分子出现N相的温度区间超过120℃.","authors":[{"authorName":"李双全","id":"e5bf21ef-0e7c-41d3-912c-003a7595fd07","originalAuthorName":"李双全"},{"authorName":"沈冬","id":"77c289bd-ab0e-45de-95a1-e4b3fd3c3bd9","originalAuthorName":"沈冬"}],"doi":"10.3788/YJYXS20112604.0421","fpage":"421","id":"73dafbde-7ee5-435a-b458-c38444e07bbb","issue":"4","journal":{"abbrevTitle":"YJYXS","coverImgSrc":"journal/img/cover/YJYXS.jpg","id":"72","issnPpub":"1007-2780","publisherId":"YJYXS","title":"液晶与显示   "},"keywords":[{"id":"f6ab93d4-d562-4015-9976-89e307552d4f","keyword":"1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"1,3,4-噻二唑"},{"id":"2799b8b9-8a19-4e23-a435-f838fb8c9f8b","keyword":"弯曲型分子","originalKeyword":"弯曲型分子"},{"id":"2dd6a720-32dc-43d9-adb8-085cd79c5716","keyword":"向列相","originalKeyword":"向列相"}],"language":"zh","publisherId":"yjyxs201104001","title":"<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>类弯曲型液晶分子的合成和性能研究","volume":"26","year":"2011"},{"abstractinfo":"采用失重法,电化学阻抗谱和极化曲线研究了碳钢在含不同浓度呋喃甲醛[5-(对<span style=\"color:red\">甲基</span>苯基)-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>-2-巯基]-乙酰腙(FPTA)缓蚀剂的0.5 mol·L-1 H2SO4溶液中的缓蚀性能.结果表明,FPTA在硫酸溶液中有很好的缓蚀率,是一种混合型缓蚀剂.FPTA在碳钢表面的吸附符合Langmuir等温吸附曲线.通过SEM证实碳钢表面形成了一层保护膜,可以阻止酸液对碳钢的腐蚀.","authors":[{"authorName":"白永玲","id":"e66a16f1-52c1-413e-a642-f51046b0510e","originalAuthorName":"白永玲"},{"authorName":"李伟华","id":"aeb0b753-360b-4a3b-8569-90d1610ca6d9","originalAuthorName":"李伟华"}],"doi":"","fpage":"150","id":"6ce5ef94-7b0e-4099-9e69-0f5261f1c146","issue":"2","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"ddc0e69d-ff5d-4248-b5e1-1e12d116eac3","keyword":"碳钢","originalKeyword":"碳钢"},{"id":"fb528ace-7462-477f-bde1-dc4aa6c84df4","keyword":"硫酸","originalKeyword":"硫酸"},{"id":"6f1dcb39-5f8e-4711-ba3f-205abc735401","keyword":"电化学","originalKeyword":"电化学"},{"id":"0b222c0e-7b07-48cb-8061-b225affdbf99","keyword":"SEM","originalKeyword":"SEM"},{"id":"e21b2a4f-1fc2-4156-ab6a-f7fa9592b95a","keyword":"缓蚀性能","originalKeyword":"缓蚀性能"}],"language":"zh","publisherId":"fsyfh201402011","title":"呋喃甲醛[5-(对<span style=\"color:red\">甲基</span>苯基)-1,3,4-<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>-2-巯基]-乙酰腙在硫酸溶液中对碳钢的缓蚀作用","volume":"35","year":"2014"},{"abstractinfo":"1-苯基-3-<span style=\"color:red\">甲基</span>-5-氯-4-吡唑甲醛与4-氨基-5-取代苯基-1,2,4-三<span style=\"color:red\">唑</span>-3-硫酮缩合生成4-(1-苯基-3-<span style=\"color:red\">甲基</span>-5-氯吡唑次甲亚胺基)-5-(取代苯基)-2H-1,2,4-三<span style=\"color:red\">唑</span>-3(4H)-硫酮,再烷基加成化为新型含吡唑基5,6-2H-1,2,4-三<span style=\"color:red\">唑</span>[3,4-b][1,3,4]<span style=\"color:red\">噻</span><span style=\"color:red\">二</span>嗪衍生物.化合物结构经1H NMR、IR以及元素分析确认.初步生物活性测试结果表明,在100 mg/L浓度下,化合物8a(3-(2-<span style=\"color:red\">甲基</span>苯基)-6-(5-氯-2-<span style=\"color:red\">甲基</span>4-苯基吡唑)-7-(4-硝基苯基)-5H-1,2,4-三<span style=\"color:red\">唑</span>[3,4-b][1,3,4]<span style=\"color:red\">噻</span><span style=\"color:red\">二</span>嗪)对黄瓜炭疽病的抑制率达90％.","authors":[{"authorName":"郑玉国","id":"b696fef1-4152-4b2f-b8c0-9e9ac182e583","originalAuthorName":"郑玉国"},{"authorName":"郭晴晴","id":"e1e210d3-f96b-4773-a4c0-2b11ecc0ee1f","originalAuthorName":"郭晴晴"},{"authorName":"周莉","id":"f2a26d34-9356-42a8-a6c4-83ac1b1bd944","originalAuthorName":"周莉"},{"authorName":"李世杰","id":"ac302c30-cb8f-4537-93a1-c34955cf2b8c","originalAuthorName":"李世杰"},{"authorName":"余忠林","id":"00c4a2f5-3c8e-4c0a-8034-02c18c18faa6","originalAuthorName":"余忠林"},{"authorName":"刘翠菊","id":"35a4d34b-ce42-4cc7-a47e-0700282f2e58","originalAuthorName":"刘翠菊"},{"authorName":"熊香","id":"d315d33a-3467-4f52-b626-6390444660a2","originalAuthorName":"熊香"}],"doi":"10.11944/j.issn.1000-0518.2015.02.140163","fpage":"151","id":"6cbdc434-1543-400e-bcd0-825ef64a281e","issue":"2","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"aba77f0c-9099-4b80-a89d-a5fcb99aa207","keyword":"吡唑","originalKeyword":"吡唑"},{"id":"d164eb86-7c8c-459a-aa9e-3624b4b2aea6","keyword":"三<span style=\"color:red\">唑</span>[3,4-b][1,3,4]<span style=\"color:red\">噻</span><span style=\"color:red\">二</span>嗪","originalKeyword":"三唑[3,4-b][1,3,4]噻二嗪"},{"id":"7e0b727b-a022-41f7-9721-4be01e4751b0","keyword":"合成","originalKeyword":"合成"},{"id":"caecc975-fe6f-4b19-88c2-e7055ddcbdae","keyword":"生物活性","originalKeyword":"生物活性"}],"language":"zh","publisherId":"yyhx201502004","title":"含吡唑1,2,4-三<span style=\"color:red\">唑</span><span style=\"color:red\">噻</span><span style=\"color:red\">二</span>嗪衍生物的合成及抑菌活性","volume":"32","year":"2015"},{"abstractinfo":"以四丁基溴化铵为相转移催化剂,2-氯-噻吩和多聚甲醛、浓盐酸进行氯<span style=\"color:red\">甲基</span>化反应生成2-氯-3-氯<span style=\"color:red\">甲基</span>-噻吩,其结构经GC-MAS、IR、1H NMR分析确定,产率为77.6 %. 2-氯-3-氯<span style=\"color:red\">甲基</span>-噻吩和1-(2,4-<span style=\"color:red\">二</span>氯苯基)-2-(1-咪唑基)-乙醇在相转移催化条件下进行O-烷基化反应,然后与浓硝酸成盐生成<span style=\"color:red\">噻</span>康<span style=\"color:red\">唑</span>,其结构经IR、1H NMR确定,产率为53%.","authors":[{"authorName":"王明慧","id":"86cb76e5-6547-401c-930c-0617a218dbfd","originalAuthorName":"王明慧"},{"authorName":"吴坚平","id":"3dee2080-848c-4150-8a0d-07e6f32720d1","originalAuthorName":"吴坚平"},{"authorName":"杨立荣","id":"f7e21ffb-2779-4f74-b9dd-4605a323d5de","originalAuthorName":"杨立荣"},{"authorName":"陈新志","id":"0d9c1d2c-5cc1-4715-968c-c24015ae4322","originalAuthorName":"陈新志"}],"doi":"10.3969/j.issn.1000-0518.2006.01.022","fpage":"106","id":"c7d576c4-1b26-4b62-a15f-bf325abea1f5","issue":"1","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"a10a4b08-09ca-41d6-9958-fd0a313e0429","keyword":"相转移催化","originalKeyword":"相转移催化"},{"id":"ac196d19-f170-492b-ade8-428435282813","keyword":"氯氯<span style=\"color:red\">甲基</span>噻吩","originalKeyword":"氯氯甲基噻吩"},{"id":"39fb55cc-dc13-4980-b958-4058adc4ab44","keyword":"氯<span style=\"color:red\">甲基</span>化","originalKeyword":"氯甲基化"},{"id":"3e4b1c3c-c663-44c0-bb6a-a6c61bab74ce","keyword":"<span style=\"color:red\">噻</span>康<span style=\"color:red\">唑</span>","originalKeyword":"噻康唑"}],"language":"zh","publisherId":"yyhx200601022","title":"相转移催化法合成2-氯-3-氯<span style=\"color:red\">甲基</span>-噻吩及<span style=\"color:red\">噻</span>康<span style=\"color:red\">唑</span>","volume":"23","year":"2006"},{"abstractinfo":"将硫代对称<span style=\"color:red\">二</span>氨基脲(1)、3-烷基-4-氨基-5-巯基-1,2,4-均三<span style=\"color:red\">唑</span>(2)和双1,2,4-均三<span style=\"color:red\">唑</span>(5)在三氯氧磷存在下分别与香豆素-3-羧酸或苯并呋喃-2-甲酸等杂环羧酸缩合关环,得到了7种含香豆素和呋喃的均三<span style=\"color:red\">唑</span>并<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>多杂环化合物,产率为57%～70%.利用元素分析、MS、IR、1H NMR对化合物进行了表征.","authors":[{"authorName":"孙一峰","id":"fa11fce0-e6a4-4cc1-9aaf-fa1414fd72ec","originalAuthorName":"孙一峰"},{"authorName":"李汴洋","id":"bb1fbcb7-47cc-4584-ba52-44dbb36dabc2","originalAuthorName":"李汴洋"},{"authorName":"宋化灿","id":"edf7b4a0-9648-4c64-9aba-cd4b1c05792f","originalAuthorName":"宋化灿"}],"doi":"10.3969/j.issn.1000-0518.2005.03.020","fpage":"316","id":"d878f7b2-2d56-4124-982e-c8500c2b80d0","issue":"3","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"417eec68-4467-4903-bfc9-223b3fd8aff1","keyword":"香豆素","originalKeyword":"香豆素"},{"id":"f4fea6db-a4c1-4bfb-8f6b-3b90d4b0adc3","keyword":"呋喃","originalKeyword":"呋喃"},{"id":"778edda4-d78d-4d6c-ace9-58423b6e864d","keyword":"均三<span style=\"color:red\">唑</span>并<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>","originalKeyword":"均三唑并噻二唑"},{"id":"d81eff7f-4537-4a9e-ab20-a65cab167a4c","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx200503020","title":"香豆素和呋喃均三<span style=\"color:red\">唑</span>并<span style=\"color:red\">噻</span><span style=\"color:red\">二</span><span style=\"color:red\">唑</span>化合物的合成","volume":"22","year":"2005"}],"totalpage":3585,"totalrecord":35844}