{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"固体恸硝酰硝酸钌不含卤素、硫、磷等惦愌起催化剂中毒的元素，是制备用于煤化工行惄的负载型钌催化剂的理想前驱体。惣水合三氯化钌为原料，通过愌入恸硝酰基、除去氯离子、萃取提纯制备了固体恸硝酰硝酸钌，适于固体恸硝酰硝酸钌的规模化合成生产。","authors":[{"authorName":"常桥稳","id":"55828985-a2ec-4ba2-880c-1be40ff58595","originalAuthorName":"常桥稳"},{"authorName":"周悀","id":"0d4547c6-5abf-4b68-abb8-8fcc593fdeb5","originalAuthorName":"周悀"},{"authorName":"晏彩先","id":"5b1113f4-13b0-4f2e-9078-b8b09b0eef60","originalAuthorName":"晏彩先"},{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span 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FAB+-MS、IR、1H-NMR 和电子光谱对其结构进行了测定和表征，并在Suzuki偶联反应模型上评价了其催化活性，催化转化率为70%~88%。","authors":[{"authorName":"刘桂华","id":"67a5897a-7289-4b10-9720-a9713855b247","originalAuthorName":"刘桂华"},{"authorName":"叶青松","id":"119185d6-da18-4bb4-b781-598c2a6ed4c9","originalAuthorName":"叶青松"},{"authorName":"左川","id":"f147a35f-a06f-4d9b-b832-ca40572f31bb","originalAuthorName":"左川"},{"authorName":"余娟","id":"0c0cfbfe-6909-4262-90c0-775633724182","originalAuthorName":"余娟"},{"authorName":"杨军","id":"b3fc9ede-892e-4594-b90a-44974f42e9d5","originalAuthorName":"杨军"},{"authorName":"姜婧","id":"dd5fff2d-91d2-473c-8360-98e3b10089b6","originalAuthorName":"姜婧"},{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span 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style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"94c2b1a0-fda1-4607-86b4-0c6aeb656bcc","originalAuthorName":"沈善问"},{"authorName":"周严","id":"cdf94e16-4f0c-4083-b68a-23db35715fd4","originalAuthorName":"周严"},{"authorName":"匡飞平","id":"3bd5a666-6c92-46bf-97cb-9a13aa8725f7","originalAuthorName":"匡飞平"},{"authorName":"冯洋洋","id":"4c7b75c4-bde5-483a-a2a8-49c680ae3039","originalAuthorName":"冯洋洋"},{"authorName":"许明明","id":"efd09d3e-9745-4cf8-873d-4d7c0cdef0af","originalAuthorName":"许明明"},{"authorName":"潘再富","id":"a1146e96-08fe-417f-b4d2-d505172ecc1e","originalAuthorName":"潘再富"}],"doi":"10.3969/j.issn.1004-0676.2011.04.005","fpage":"21","id":"b12ebe02-bf12-4604-bd9e-401f78712d80","issue":"4","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"d2dec0bb-d06b-48eb-a001-df8d2e782787","keyword":"冶金技术","originalKeyword":"冶金技术"},{"id":"f8cd2d7d-28e7-40dd-8dd5-1473ceb42277","keyword":"三(三苯基膦)氯化铑","originalKeyword":"三(三苯基膦)氯化铑"},{"id":"285e604a-780d-41d6-8e75-41e7998f7d2e","keyword":"废料","originalKeyword":"废料"},{"id":"b80e1164-2ba4-428d-9fb6-f474b1c7f143","keyword":"回收","originalKeyword":"回收"}],"language":"zh","publisherId":"gjs201104005","title":"从合成三(三苯基膦)氯化铑产生的有机废液中回收铑","volume":"32","year":"2011"},{"abstractinfo":"以三氯化铑为原料,在弱酸性条件下,直接与辛酸回流反应,成功制备了辛酸铑(Ⅱ),产率＞95％,产品纯度＞99.0％,适合工业化生产要求.辛酸铑(Ⅱ)样品通过质谱分析、红外光谱分析和单晶X射线衍射分析确定为二聚体,以羧基为桥联配体,形成灯笼状的空间立体结构.","authors":[{"authorName":"刘桂华","id":"6cb8ba6b-916c-4c9d-aec1-d078689e03ec","originalAuthorName":"刘桂华"},{"authorName":"叶青松","id":"36b29982-31a4-4ae9-8b50-b94f8a5e9e71","originalAuthorName":"叶青松"},{"authorName":"潘再富","id":"135534e1-66bd-4975-ae72-a560746e66bf","originalAuthorName":"潘再富"},{"authorName":"侯文明","id":"1e59be3c-f89d-47aa-be3a-4223139a0de4","originalAuthorName":"侯文明"},{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"2b1617c9-d0d6-4ca7-99b3-1c932efd12c0","originalAuthorName":"沈善问"},{"authorName":"余尧","id":"e3582b5a-ef5c-41a4-8433-8d02eb527287","originalAuthorName":"余尧"},{"authorName":"谌喜珠","id":"acbbecf9-5d2a-4ea0-99a6-cd66275b96e6","originalAuthorName":"谌喜珠"},{"authorName":"姜婧","id":"49a25456-c9f4-45ae-a06d-726e5d337497","originalAuthorName":"姜婧"},{"authorName":"刘伟平","id":"f12de0de-d139-4c89-8f91-e2c5f47100cf","originalAuthorName":"刘伟平"}],"doi":"","fpage":"18","id":"f0ce74ce-d7cb-4765-a1aa-aef82b5a4152","issue":"4","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"c62e9ac4-b782-4839-8f02-2c29380b5ac2","keyword":"有机化学","originalKeyword":"有机化学"},{"id":"8ae5a7e0-d9fe-46e2-9c5a-99027c43daa4","keyword":"辛酸铑","originalKeyword":"辛酸铑"},{"id":"679b0b2f-d8a3-4879-9a74-9c32e4613a14","keyword":"合成","originalKeyword":"合成"},{"id":"0fb9b21f-b04c-4103-90b7-fe1e6659ef37","keyword":"结构","originalKeyword":"结构"}],"language":"zh","publisherId":"gjs201204004","title":"辛酸铑(Ⅱ)的合成及其结构表征","volume":"33","year":"2012"},{"abstractinfo":"综述了制备方法、钌前驱体种类和活性炭性质时Ru/C催化剂性能的影响,阐述了Ru/C催化剂在羰基加氢和芳环加氢反应中的具体应用,并对Ru/C催化剂的开发进行了展望.","authors":[{"authorName":"戴云生","id":"91488660-b7fe-4cdf-a880-a428c53e0ae2","originalAuthorName":"戴云生"},{"authorName":"潘再富","id":"f7baeac5-9990-4947-a285-9d5fcd43de8a","originalAuthorName":"潘再富"},{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"c9775570-eebd-4ae1-8e65-a9c5a5335e53","originalAuthorName":"沈善问"},{"authorName":"<span style=\"color:red\">沈</span>亚峰","id":"60c899a6-f388-4fde-ae2d-3ce0e168aad2","originalAuthorName":"沈亚峰"},{"authorName":"左川","id":"f0f2056a-ceb0-4b76-bffe-5bd3939715e7","originalAuthorName":"左川"},{"authorName":"唐春","id":"bf723299-78b2-4ad6-9d82-01fb951065b8","originalAuthorName":"唐春"},{"authorName":"陈家林","id":"1aeb75d6-4c14-429d-afd6-aa7185e5a2e8","originalAuthorName":"陈家林"}],"doi":"10.3969/j.issn.1004-0676.2012.01.016","fpage":"84","id":"29cb2d17-5983-4fb8-b3bc-ce3c1eb42f00","issue":"1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"2ac1067f-45c0-41d5-96ef-71a63b87e621","keyword":"物理化学","originalKeyword":"物理化学"},{"id":"73dce5f5-e1a1-4100-a754-dff4b47d5b64","keyword":"Ru/C","originalKeyword":"Ru/C"},{"id":"12774b9a-f14d-4c84-8bca-4c3a4930eee1","keyword":"贵金属载体催化剂","originalKeyword":"贵金属载体催化剂"},{"id":"f703b802-fa93-4b56-92fd-a06734f71453","keyword":"羰基加氢","originalKeyword":"羰基加氢"},{"id":"a87a39e7-4e2d-4fc7-89a7-b15a4fd04d6d","keyword":"芳环加氢","originalKeyword":"芳环加氢"}],"language":"zh","publisherId":"gjs201201016","title":"Ru/C催化剂的制备及其在精细化工中的应用","volume":"33","year":"2012"},{"abstractinfo":"以醋酸钌为前驱体,用浸渍还原法制备Ru/C催化剂,以常压下葡萄糖加氢制取山梨醇的反应评价其活性,并用透射电子显微镜(TEM)及X射线衍射对其进行表征,研究了活性碳类型、温度、浸渍和还原时间、pH值、不同前驱体及有机助剂的加入等因素对Ru/C催化剂活性的影响.结果表明,适当的活性碳粒度、大的比表面和孔容有利于Ru粒子在活性碳表面均匀分布,提高催化活性.80~90℃的温度,8~10h的浸渍时间,6~8h还原时间及7~8的pH值有利于Ru粒子在活性碳载体上形成高分散、高活性的Ru/C催化剂.加入有机助剂使催化剂活性明显高于没有加入有机助剂的催化剂.不同的前驱体对Ru/C催化剂在该反应中的催化活性有较大的影响,醋酸钌是一种制备Ru/C催化剂较好的前驱体.","authors":[{"authorName":"<span style=\"color:red\">沈</span>亚峰","id":"c4226d8b-d1b3-4982-9c06-9bde3ad93423","originalAuthorName":"沈亚峰"},{"authorName":"雷远进","id":"dd5fadf0-ff7d-4c82-9910-b542737ff5f4","originalAuthorName":"雷远进"},{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"c6122ad3-bca6-4df6-bc59-cdf3deae05c7","originalAuthorName":"沈善问"},{"authorName":"潘再富","id":"be950adf-0344-4aa1-8cc1-05e2cef666a9","originalAuthorName":"潘再富"}],"doi":"10.3969/j.issn.1004-0676.2009.01.008","fpage":"40","id":"1f618e5f-99b1-4de1-b371-4c572ea1ab56","issue":"1","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"98c7b032-a2ac-4be4-89d8-5083d076bd30","keyword":"物理化学","originalKeyword":"物理化学"},{"id":"0b68a366-fd81-4899-bfdb-d2b818920fc6","keyword":"醋酸钌","originalKeyword":"醋酸钌"},{"id":"de7e86dd-b8a0-454d-ba05-ed662f05f4d3","keyword":"Ru/C","originalKeyword":"Ru/C"},{"id":"28548fe2-06b6-44bb-87bb-397458c2dcaa","keyword":"葡萄糖加氢","originalKeyword":"葡萄糖加氢"},{"id":"fcab19c6-7c1a-496d-8bc7-60e7e793761c","keyword":"碘量滴定法","originalKeyword":"碘量滴定法"}],"language":"zh","publisherId":"gjs200901008","title":"以醋酸钌为前驱体的Ru/C催化剂在葡萄糖加氢制取山梨醇反应中活性的研究","volume":"30","year":"2009"},{"abstractinfo":"采用氯酸钾作助熔剂，经过高频燃烧后，用红外碳硫仪测定纯银及银基合金中的微量碳、硫，测定范围碳：0.005%~0.12%，硫：0.005%~0.099%。方法准确度高，相对标准偏差、加标回收率分别为碳：3.3%~10.9%、91%~120%；硫：2.8%~10%、91%~120%。","authors":[{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"ad90f6d8-42e9-43a8-b5f5-b72aaed11b18","originalAuthorName":"沈善问"}],"doi":"","fpage":"66","id":"f8fc674c-aeee-4fff-ad2c-b6adbf985aea","issue":"2","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"9e56fea2-c739-46e9-82df-1fd1c77a2c70","keyword":"分析化学","originalKeyword":"分析化学"},{"id":"f7a1b983-32c1-44ab-96ae-45ec0aa9cbab","keyword":"高频燃烧-红外吸收","originalKeyword":"高频燃烧-红外吸收"},{"id":"ce7f41cb-6db4-45a6-b2fb-ad8e96322bc5","keyword":"银及银合金","originalKeyword":"银及银合金"},{"id":"7aa6f65e-76ec-4a0c-9c2e-f297b18dc64b","keyword":"碳","originalKeyword":"碳"},{"id":"33f343d0-c9e2-454a-960f-474656a029e4","keyword":"硫","originalKeyword":"硫"}],"language":"zh","publisherId":"gjs201502014","title":"高频燃烧红外吸收法测定纯银及银合金中微量的碳硫","volume":"","year":"2015"},{"abstractinfo":"在 N,N-二甲基甲酰胺介质中，将水合三氯化铑与乙酰丙酮加热回流，一步合成了乙酰丙酮·二羰基铑([Rh(CO)2(acac)]2)，产率为93%；以正丁烷为介质，[Rh(CO)2(acac)]2与三苯基磷(PPh3)定量反应，得到乙酰丙酮·三苯基膦·羰基铑(Rh(acac)(PPh3)(CO))，产率为99%。用气相扩散法和溶剂缓慢挥发法分别培养出[Rh(CO)2(acac)]2和 Rh(acac)(PPh3)(CO)单晶，元素分析的结果表明产物为目标化合物。用X射线单晶衍射仪对其结构进行了表征，获得了晶体结构参数，结果表明2种化合物均为三斜晶系、P-1空间群，[Rh(CO)2(acac)]2为二聚体化合物，Rh(acac)(PPh3)(CO)为单核配合物。","authors":[{"authorName":"余娟","id":"6c839ae9-0bac-4a26-88c5-1b518a823c30","originalAuthorName":"余娟"},{"authorName":"叶青松","id":"09c86c6d-cec2-4ae6-8a0b-26a71c763dae","originalAuthorName":"叶青松"},{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"f1d44bc5-d742-4174-b5bc-4642d52aaa0c","originalAuthorName":"沈善问"},{"authorName":"左川","id":"0ebe3da2-cb60-4f74-b011-7fe4064020bc","originalAuthorName":"左川"},{"authorName":"刘桂华","id":"75e57c46-653d-4f7b-996d-c24ac02dfbf6","originalAuthorName":"刘桂华"},{"authorName":"刘伟平","id":"03bbb03e-5fe8-4f43-b919-1bdd38f4ef7c","originalAuthorName":"刘伟平"}],"doi":"","fpage":"8","id":"242afdc6-152c-47a2-9681-f8de9473d346","issue":"2","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"e2609b7e-04b5-4028-a700-a3402215cf0e","keyword":"有机化学","originalKeyword":"有机化学"},{"id":"e711265f-f8fb-4ae6-b7af-bdbc4fe85d7e","keyword":"乙酰丙酮·二羰基铑","originalKeyword":"乙酰丙酮·二羰基铑"},{"id":"05f41fff-7720-461f-bc3a-22fc330da3e6","keyword":"乙酰丙酮·三苯基膦·羰基铑","originalKeyword":"乙酰丙酮·三苯基膦·羰基铑"},{"id":"020f61f1-7b6b-4001-b762-1b08fc56b58a","keyword":"合成","originalKeyword":"合成"},{"id":"68ddd603-dafe-44c4-b64e-9ad7532b8dec","keyword":"晶体结构","originalKeyword":"晶体结构"}],"language":"zh","publisherId":"gjs201602002","title":"两种乙酰丙酮·羰基铑化合物的合成与晶体结构表征","volume":"37","year":"2016"},{"abstractinfo":"采用HCS-140型红外吸收碳硫分析仪同时测定贵金属催化剂中的碳、硫含量.试验了助熔剂种类、用量、样品量对测定的影响,用异标校正测定了多种类型贵金属催化剂中的碳、硫.取得了满意结果,方法的相对标准偏差为0.2%～7.7%.","authors":[{"authorName":"<span style=\"color:red\">沈</span><span style=\"color:red\">善</span><span style=\"color:red\">问</span>","id":"d9dd9d1a-1b0a-4291-bf2d-532b5db5732f","originalAuthorName":"沈善问"},{"authorName":"邱红莲","id":"ca5208df-649d-4ee1-b531-740b0f737d40","originalAuthorName":"邱红莲"},{"authorName":"刘继升","id":"63536fc7-33e5-4278-941c-06d89570e9d9","originalAuthorName":"刘继升"}],"doi":"10.3969/j.issn.1004-0676.2001.03.010","fpage":"44","id":"4a2b210f-9ff2-4406-b50d-4f082f28a121","issue":"3","journal":{"abbrevTitle":"GJS","coverImgSrc":"journal/img/cover/GJS.jpg","id":"38","issnPpub":"1004-0676","publisherId":"GJS","title":"贵金属"},"keywords":[{"id":"4b508757-4162-4484-9d23-bf7d44ea4d6f","keyword":"红外吸收法","originalKeyword":"红外吸收法"},{"id":"41d81690-cd8d-4018-bfcd-e3392716c180","keyword":"贵金属催化剂","originalKeyword":"贵金属催化剂"},{"id":"ea297c34-2e94-49d3-bfb3-4ad6fce5330b","keyword":"碳","originalKeyword":"碳"},{"id":"c56f5ba8-aa24-46c7-a7c4-0bf11f3094a3","keyword":"硫","originalKeyword":"硫"}],"language":"zh","publisherId":"gjs200103010","title":"高频红外吸收法测定贵金属催化剂中的碳、硫","volume":"22","year":"2001"},{"abstractinfo":"<正> <span style=\"color:red\">问</span>:吹入空气的100℃40%醋酸中,可使用304钢吗? 答:在100℃醋酸水溶液中,SUS304钢的耐蚀性虽因醋酸浓度不同而有一些差别,但不明显。一方面,在同样条件下吹入空气时,耐蚀性显著改善。可是当不纯物的Cl~-,以ppm数量级混入时,醋酸的腐蚀性急剧变强。这样,在醋酸环境下","authors":[{"authorName":"李自强","id":"fab31630-3fd8-4151-81a3-e3d42d80a840","originalAuthorName":"李自强"}],"categoryName":"|","doi":"","fpage":"5","id":"6107a917-1a80-4ca9-b4bc-4d89b72543f2","issue":"2","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[],"language":"zh","publisherId":"1002-6495_1989_2_10","title":"有<span style=\"color:red\">问</span>有答","volume":"1","year":"1989"}],"totalpage":28,"totalrecord":273}