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Thermal Stability of Non-Equilibrius Microstructure in Microalloyed Steel During Reheating

H.B. Wu , H.T. Jiang , S.W. Yang , D. Tang , X.L. He , null

金属学报(英文版)

Cooled in water after isothermal relaxation of deformed austenite for different times, an Nb-bearing microalloyed steel always exhibits synthetic microstructures, in which bainitic ferrite dominates. Dislocation configurations and distributions of strain induced precipitates inside bainitic ferrite of samples relaxed for different times were distinct. When compared with the austenite model steel, which maintained fcc structure even at room temperature, the strain induced precipitates were not found in the sample without relaxation whereas these were distributed outside dislocations in sample relaxed for 1000s. Most of the strain induced precipitates distribute along dislocations and pin dislocations in sample relaxed for appropriate time. After bainitic transformation, the dislocations formed in deformed austenite remain to be pinned by the precipitates. When these samples were reheated to and held at 650 or 700¡æ, the non-equilibrious microstructures tended to evolve into equilibrious ones. The sample relaxed for 60s displayed the highest thermo-stability, whereas microstructure evolution was the quickest in the sample relaxed for 1000s even though it was the softest prior to reheating. Dislocations inside laths got rid of pinning of precipitates, and their polygonization became the precursor to the evolution of microstructures during reheated and held, followed by gradual disappearance of lath boundaries caused by dislocation climbing. Finally, recrystallization occurred and polygonal ferrite appeared. By hardness measurement, it was found that softening is not a single process occurring during reheated, in which hardness fluctuates with time. There were two peaks in the hardness-time curve of each sample having undergone relaxation, while single peak occured in the curve of the sample not being relaxed. These results indicated that the thermo-stability of microstructures was determined by their history of formation to a considerable degree.

关键词: bainite , null , null , null

Al-Zn-Mg-Cu合金第二相粒子及其无析出区与晶界的作用过程研究

贺永东 , 陈明安 , 张新明

稀有金属材料与工程

制备一种含Sc和一种含Cr、Mn、Ti、Zr的Al-Zn-Mg-Cu合金,采用透射电镜研究合金中第二相粒子周围的无析出微区和晶界上的无沉淀析出带及其相互的作用过程,给出单个第二相粒子对晶界作用力的方程.当驱使晶界迁移的动力大于粒子及其周围的无析出微区对晶界的阻碍作用时,晶界被粒子穿透而形成孔洞.在晶界扫过粒子的过程中,经历了先加速后减速两个阶段.晶界位于粒子直径区位置时所受的阻力最小、运动速度最大.当晶界能与相界能增量之和等于晶界运动的驱动力时,晶界被粒子钉扎而停止运动.在晶界迁移的过程中,溶质原子倾向于由高浓度区域向低浓度区域扩散,晶界和粒子周围的无析出区对晶界的迁移过程有明显的影响.

关键词: Al-Zn-Mg-Cu合金 , 粒子 , 晶界 , 扩散 , 钉扎 , 无析出区

中子辐照6H-SiC晶体中的钉扎效应

阮永丰 , 马鹏飞 , 贾敏 , 李文润 , 张宇晖 , 张守超 , 王丹丽

人工晶体学报

分别对两种不同的6H-SiC晶体进行了总通量为5.74×10~(18) n· cm~(-2)、8.2×10~(18) n· cm~(-2)和1.72×10~(19) n· cm~(-2)的不同剂量的中子辐照,利用X射线衍射等手段观测了中子辐照引起的晶体内部损伤.结果表明:两种样品在不同的中子通量辐照下,消除部分原始缺陷的、纯度较高的样品辐照后的内部损伤明显小于纯度较低、内部原始缺陷较多的样品.样品的辐照损伤不仅取决于中子辐照剂量,还取决于其辐照时的成分和结构.晶体的结构缺陷和杂质,作为一种"钉扎",在辐照过程中作用极大,它们导致了晶体的长程缺陷(如位错)的大幅度增加.

关键词: SiC , 中子辐照 , 辐照缺陷 , 钉扎

BaNi0.1Fe1.9As2单晶的钉扎机制及涡旋相图

鲁俊超 , 于景新

低温物理学报

本文中,我们通过磁-电阻测量研究了Tc=19.4K的BaNi0.1Fe1.9As2单晶中的涡旋玻璃-涡旋液体相变.根据修正过的涡旋玻璃理论,并通过选择合适的临界指数s和H0,我们对所有的ρ(H,T)电阻曲线进行了标度,并得到了很好的结果.基于涡旋玻璃温度Tg,涡旋维度转变温度T*和上临界磁场Hc2,我们得到了H⊥c和H//c两个磁场方向的涡旋相图.结果表明,磁场低于和高于5T,钉扎机制由单涡旋钉扎和集体蠕动共存转变为集体蠕动.

关键词: 铁基超导体 , 磁-电阻 , 钉扎 , 相变

高温超导磁悬浮轴承的发展现状及前景

许吉敏 , 张飞 , 金英泽 , 张帆 , 袁小阳

中国材料进展 doi:10.7502/j.issn.1674-3962.2017.05.01

第二类高温超导体的磁通钉扎效应使得超导体在外加磁场中无需主动控制而能稳定悬浮.利用这种无源自稳定悬浮特性,高温超导磁悬浮轴承可以实现部件之间无机械摩擦的高速相对运动,在旋转机械、飞轮储能和交通运输等方面展现出了良好的应用前景.近年来,高温超导磁悬浮轴承的发展在世界范围内取得了令人瞩目的成就,轴承的设计思想、结构和应用环境都得到了相应的拓展.从结构特征角度综述了近年来国内外超导磁悬浮轴承样机的发展现状,重点介绍了西安交通大学的超导磁液复合轴承结构及其在液体火箭中的应用方案;结合该领域的研究现状探讨了超导磁悬浮轴承有待研究的问题和应用前景,指出超导轴承应向复合支撑方向发展以利于推进应用.

关键词: 钉扎 , 无源自稳定 , 高温超导磁悬浮轴承 , 发展现状 , 应用前景

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